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Federal Highway Administration Research and Technology
Coordinating, Developing, and Delivering Highway Transportation Innovations

Report
This report is an archived publication and may contain dated technical, contact, and link information
Publication Number: FHWA-HRT-04-111
Date: February 2005

Evaluation of The Laboratory Asphalt Stability Test

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APPENDIX B
Data of Separation Ratios and Degradation Ratios on Replicates

Data deviating significantly from the average are highlighted.

Table 35. SBS-rg (B6231) degradation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

HT

HT

HT

HT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

1.50

0.95

1.00

0.99

1.10

0.90

0.83

0.97

1.05

1.03

1.00

1.02

0.58

0.91

0.98

0.98

2.04

0.94

1.05

0.98

1.16

0.87

0.86

0.97

1.38

1.03

1.06

1.02

1.04

1.01

1.04

0.97

24 hour

1.31

0.94

1.01

0.97

1.05

0.92

0.82

0.97

1.19

1.00

1.13

0.98

1.01

1.01

1.02

0.94

1.31

0.94

1.04

0.98

1.00

0.91

0.86

0.98

1.11

1.00

1.08

1.00

0.92

1.01

1.01

0.96

31 hour

1.31

0.94

-

-

0.99

0.91

-

-

1.10

0.99

-

-

0.79

1.00

-

-

1.28

0.94

-

-

0.96

0.92

-

-

1.14

1.00

-

-

1.00

1.01

-

-

48 hour

1.31

0.94

1.06

0.96

0.97

0.92

0.85

0.97

1.17

0.98

1.18

0.95

0.95

1.01

1.01

0.93

1.40

0.94

1.05

0.96

0.99

0.91

0.85

0.97

2.29

0.97

1.14

0.94

0.85

1.01

0.98

0.93


Table 36. EVA (B6232) separation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

0.97

0.99

0.93

1.01

1.02

0.99

1.01

1.00

0.93

0.95

0.85

1.02

1.08

1.00

1.09

1.00

6 hour

0.78

1.00

0.78

1.06

0.60

1.04

0.65

1.08

0.98

0.99

0.96

1.01

1.13

1.01

1.12

1.01

0.58

1.01

0.58

1.11

1.13

0.99

1.11

0.97

0.90

1.00

1.01

1.00

0.97

0.99

0.96

1.00

0.61

1.01

0.60

1.11

0.56

1.05

0.61

1.08

-

-

-

-

-

-

-

-

24 hour

0.79

1.01

0.81

1.05

0.81

1.01

0.82

1.01

0.92

1.00

0.91

1.03

0.74

1.00

0.74

1.00

0.69

1.01

0.70

1.07

0.37

1.05

0.41

1.12

1.03

1.00

1.03

1.00

0.93

0.99

0.92

0.99

31 hour

0.50

0.97

0.47

1.13

0.97

0.98

0.95

0.99

-

-

-

-

-

-

-

-

0.62

1.01

0.63

1.09

0.75

0.99

0.75

1.00

-

-

-

-

-

-

-

-

0.55

1.01

0.55

1.11

0.33

1.06

0.37

1.13

-

-

-

-

-

-

-

-

48 hour

0.51

1.03

0.50

1.14

0.87

0.98

0.83

0.97

0.88

0.98

0.87

1.03

1.11

1.01

1.15

1.01

0.63

1.00

0.63

1.09

0.81

1.04

0.85

1.03

0.96

1.27

0.95

1.26

1.12

0.98

1.09

0.97

0.72

0.97

0.69

1.07

0.85

0.99

0.84

1.00

-

-

-

-

-

-

-

-

Table 37. EVA (B6232) degradation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

0.98

1.00

0.98

1.00

0.72

1.03

0.77

1.06

1.09

1.02

1.10

0.98

0.81

1.01

0.85

1.02

0.41

0.49

0.40

0.52

0.64

1.02

0.68

1.06

1.14

1.02

1.16

0.97

0.92

1.02

0.95

1.03

-

-

-

-

1.26

0.99

1.23

0.98

-

-

-

-

-

-

-

-

24 hour

0.39

0.50

0.40

0.52

0.90

1.01

0.93

1.02

1.16

1.02

1.18

0.97

0.88

1.00

0.88

1.00

0.93

1.01

0.95

1.01

1.14

0.99

1.37

0.99

1.20

1.02

1.20

0.96

0.91

1.02

0.93

1.02

1.09

1.01

1.11

0.98

-

-

-

-

-

-

-

-

-

-

-

-

31 hour

1.24

0.99

1.25

0.98

0.76

1.02

0.80

1.04

-

-

-

-

-

-

-

-

1.12

1.00

1.13

0.98

0.74

1.02

0.78

1.03

-

-

-

-

-

-

-

-

1.19

1.01

1.21

0.98

1.56

0.98

1.48

0.97

-

-

-

-

-

-

-

-

48 hour

1.25

0.99

1.26

0.97

0.84

1.00

0.86

1.02

1.20

1.00

1.18

0.96

0.88

1.00

0.89

1.01

1.19

0.99

1.14

0.94

0.74

1.02

0.78

1.05

1.27

1.01

1.26

0.95

0.94

1.00

0.94

1.00

1.02

0.99

1.00

1.00

0.74

1.02

0.79

1.05

-

-

-

-

-

-

-

-


Table 38. EVA (B6232) separation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

0.97

0.99

-

-

0.93

1.01

-

-

6 hour

0.78

1.00

0.74

1.01

0.78

1.06

0.74

1.00

0.58

1.01

-

-

0.58

1.11

-

-

0.61

1.01

-

-

0.60

1.11

-

-

24 hour

0.79

1.01

0.57

1.01

0.81

1.05

0.57

0.98

0.69

1.01

0.52

1.01

0.70

1.07

0.51

0.98

31 hour

0.50

0.97

-

-

0.47

1.13

-

-

0.62

1.01

-

-

0.63

1.09

-

-

0.55

1.01

-

-

0.55

1.11

-

-

48 hour

0.51

1.03

-

-

0.50

1.14

-

-

0.63

1.00

0.52

1.01

0.63

1.09

0.51

0.99

0.72

0.97

0.56

1.00

0.69

1.07

0.55

0.97

Table 39. EVA (B6232) degradation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

-

-

1.00

1.00

-

-

6 hour

0.98

1.00

0.89

0.99

0.98

1.00

0.89

0.98

0.41

0.49

-

-

0.40

0.52

-

-

-

-

-

-

-

-

-

-

24 hour

0.39

0.50

1.05

0.99

0.40

0.52

1.05

1.00

0.93

1.01

1.07

0.99

0.95

1.01

1.07

0.99

1.09

1.01

-

-

1.11

0.98

-

-

31 hour

1.24

0.99

-

-

1.25

0.98

-

-

1.12

1.00

-

-

1.13

0.98

-

-

1.19

1.01

1.04

0.99

1.21

0.98

1.03

0.99

41 hour

1.25

0.99

1.06

0.99

1.26

0.97

1.05

0.99

1.19

0.99

-

-

1.14

0.94

-

-

1.02

0.99

-

-

1.00

1.00

-

-

Table 40. EVA-g (B6233) separation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

0.99

1.00

0.99

1.00

1.03

1.01

1.06

1.01

0.98

1.00

0.97

1.01

1.07

0.98

1.05

0.98

6 hour

0.87

1.01

0.88

1.03

0.79

1.03

0.83

1.04

0.90

1.00

0.94

1.03

0.99

1.00

0.99

1.00

0.93

1.00

0.94

1.02

0.67

1.02

0.70

1.04

1.01

1.00

1.02

0.99

0.94

0.99

0.93

1.00

24 hour

0.69

1.03

0.75

1.10

0.76

1.04

0.81

1.06

0.87

1.03

0.93

1.04

1.14

1.01

1.16

1.01

0.81

1.02

0.83

1.05

0.48

1.05

0.52

1.09

0.95

1.00

0.97

1.01

1.04

1.00

1.04

1.00

31 hour

0.78

1.01

0.80

1.06

0.81

0.99

0.80

0.77

0.97

1.00

0.99

1.00

0.94

1.01

0.95

1.01

0.71

1.01

0.73

1.08

0.58

1.02

0.61

1.06

1.02

1.00

1.02

0.99

1.14

1.00

1.14

1.00

48 hour

0.78

1.01

0.80

1.06

0.45

1.03

0.48

1.06

1.02

1.00

1.02

1.00

0.66

1.00

0.66

0.99

0.66

1.01

0.70

1.09

0.35

1.11

0.42

1.29

1.03

1.00

1.05

0.99

1.12

1.01

1.13

1.02

Table 41. EVA-g (B6233) degradation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

1.04

1.00

1.04

0.99

0.84

1.03

0.88

1.03

0.91

1.00

0.93

1.03

0.94

1.00

0.94

1.00

1.03

1.00

1.02

0.99

1.00

1.00

1.01

1.01

0.97

1.00

0.97

1.01

0.91

1.01

0.93

1.01

24 hour

1.14

0.99

1.09

0.97

0.88

1.02

0.90

1.03

1.10

0.98

1.05

0.97

0.83

1.00

0.83

1.00

1.15

0.99

1.11

0.97

1.26

1.00

1.23

0.99

0.98

1.00

0.97

1.01

0.97

0.99

0.97

1.00

31 hour

1.12

0.99

1.07

0.98

0.74

1.01

0.77

1.05

1.05

0.99

1.03

0.98

0.89

1.00

0.90

1.01

1.17

0.99

1.14

0.97

0.97

1.02

1.01

1.04

1.03

1.00

1.01

0.99

0.87

1.03

0.92

1.04

48 hour

1.14

0.99

1.11

0.96

1.16

0.99

1.14

1.00

1.09

0.99

1.04

0.98

0.84

0.99

0.83

1.00

1.27

0.99

1.22

0.95

1.34

0.99

1.29

1.00

1.07

0.99

1.04

0.98

0.90

1.00

0.92

1.01

Table 42. EVA-g (B6233) separation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

1.03

1.01

1.06

1.00

1.06

1.01

1.06

1.00

6 hour

0.79

1.03

0.89

1.02

0.83

1.04

0.90

1.02

0.67

1.02

0.80

1.02

0.70

1.04

0.83

1.02

24 hour

0.76

1.04

0.82

1.04

0.81

1.06

0.84

1.02

0.48

1.05

0.59

1.04

0.52

1.09

0.63

1.08

31 hour

0.81

0.99

1.09

0.98

0.80

0.77

1.72

0.96

0.58

1.02

0.34

1.09

0.61

1.06

0.39

1.15

48 hour

0.45

1.03

0.53

1.04

0.48

1.06

0.58

1.08

0.35

1.11

0.26

1.08

0.42

1.29

0.31

1.18

Table 43. EVA-g (B6233) degradation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

Time of
Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

0.84

1.03

0.84

1.02

0.88

1.03

0.88

1.04

1.00

1.00

1.02

1.02

1.01

1.01

1.05

1.02

24 hour

0.88

1.02

0.65

1.03

0.90

1.03

0.70

1.07

1.26

1.00

0.85

1.08

1.23

0.99

0.90

1.05

31 hour

0.74

1.01

0.71

1.02

0.77

1.05

0.61

1.06

0.97

1.02

1.29

1.00

1.01

1.04

1.27

1.01

48 hour

1.16

0.99

0.87

1.01

1.14

1.00

0.89

1.03

1.34

0.99

1.33

1.00

1.29

1.00

1.29

1.01

Table 44. ESI (B6243) separation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

1.02

1.00

1.02

1.00

1.17

1.00

1.16

0.99

0.96

1.00

0.96

1.01

0.99

1.00

0.99

0.99

6 hour

0.95

1.00

0.95

1.02

0.69

1.05

0.76

1.09

0.93

1.02

0.99

1.01

1.07

1.04

1.17

1.07

-

-

-

-

1.22

0.98

1.17

0.96

0.86

1.08

0.95

1.03

0.98

1.01

0.99

1.00

-

-

-

-

-

-

-

-

1.03

0.99

1.02

0.99

0.79

1.02

0.84

1.05

24 hour

1.01

1.00

1.00

1.01

0.70

1.03

0.75

1.06

1.02

0.98

0.98

1.00

0.84

0.99

0.85

1.01

0.99

1.00

0.99

1.00

-

-

-

-

0.95

1.01

0.98

1.01

0.97

0.99

0.97

1.00

-

-

-

-

-

-

-

-

0.99

0.97

0.98

1.00

1.05

1.01

1.06

1.00

31 hour

0.92

1.01

0.94

1.03

0.73

1.05

0.80

1.07

1.00

1.01

1.00

1.00

1.09

0.97

1.04

0.96

0.91

1.00

0.90

1.03

0.65

1.05

0.70

1.06

1.01

1.00

1.00

1.00

1.11

0.99

1.14

0.98

-

-

-

-

-

-

-

-

1.03

1.00

1.01

1.00

0.87

1.00

0.87

1.01

48 hour

0.99

1.00

0.99

1.00

0.76

1.03

0.79

1.05

1.02

1.00

1.03

0.99

0.78

1.01

0.80

1.02

1.03

0.99

0.97

1.01

0.97

0.99

0.95

0.99

1.05

0.99

1.01

0.99

0.76

1.01

0.80

1.02

-

-

-

-

-

-

-

-

1.05

1.00

1.03

0.99

0.96

1.02

0.99

1.02

Table 45. ESI (B6243) degradation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

1.01

1.00

1.00

1.00

1.16

0.98

1.13

0.98

1.05

0.99

1.03

0.99

0.88

1.00

0.89

0.98

-

-

-

-

1.20

0.98

1.15

0.97

1.14

0.96

1.05

0.97

0.95

1.01

0.98

1.00

-

-

-

-

-

-

-

-

1.25

0.98

1.07

0.97

0.84

1.01

0.87

1.01

24 hour

1.05

0.98

1.10

0.66

1.08

0.99

1.05

0.99

1.21

0.96

1.07

0.96

0.81

1.01

0.85

1.02

1.03

0.98

1.08

0.66

-

-

-

-

1.10

1.00

1.08

0.97

0.70

1.03

0.76

1.05

-

-

-

-

-

-

-

-

1.16

0.98

1.07

0.97

0.93

1.01

0.95

0.99

31 hour

1.01

1.00

1.01

0.99

1.16

0.98

1.12

0.98

1.07

1.00

1.05

0.98

0.85

1.01

0.88

1.01

1.05

1.00

1.06

0.98

1.22

0.98

1.16

0.97

1.09

1.00

1.07

0.97

0.84

1.01

0.87

1.01

-

-

-

-

-

-

-

-

1.12

1.00

1.10

0.96

0.86

1.01

0.88

1.01

48 hour

1.15

1.00

1.11

0.95

1.05

0.98

1.02

0.98

1.15

1.00

1.12

0.96

1.01

0.99

1.02

0.99

1.21

1.00

1.16

0.94

1.03

0.97

0.99

0.98

1.24

1.00

1.18

0.94

0.85

1.00

0.87

1.00

-

-

-

-

-

-

-

-

1.15

1.01

1.14

0.95

1.05

1.00

1.06

0.99


Table 46. CMCRA (B6251) separation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

0.98

1.00

0.97

1.00

1.12

1.00

1.13

1.00

1.08

1.00

1.10

0.99

1.02

1.00

1.02

0.99

6 hour

0.84

1.02

0.90

1.05

1.12

1.02

1.14

1.01

1.08

0.99

1.07

0.98

0.98

1.01

0.99

1.01

0.84

1.01

0.90

1.04

1.05

1.01

1.05

1.00

1.01

1.00

1.00

1.00

1.03

1.00

1.03

1.03

-

-

-

-

1.04

1.00

1.05

1.00

1.08

0.97

1.07

0.98

0.93

1.00

0.94

1.00

24 hour

-

-

-

-

-

-

-

-

0.99

1.00

0.98

1.00

0.94

1.00

0.94

1.00

-

-

-

-

-

-

-

-

0.98

1.00

1.03

1.00

1.18

1.00

1.19

1.00

-

-

-

-

-

-

-

-

0.99

1.00

1.02

1.00

1.02

1.00

1.03

1.00

31 hour

0.61

1.09

0.78

1.14

1.26

1.00

1.26

0.99

0.88

1.01

0.90

1.04

0.85

1.00

0.85

1.00

0.72

1.07

0.89

1.10

1.21

1.01

1.21

1.01

0.99

1.00

0.99

1.00

0.97

1.01

0.97

1.01

0.68

1.07

0.84

1.11

1.14

1.01

1.14

1.00

-

-

-

-

0.99

1.00

0.98

1.00

48 hour

0.72

1.08

0.89

1.09

1.23

1.00

1.23

0.99

0.98

1.00

0.97

1.01

0.96

1.00

0.96

1.00

0.64

1.11

0.92

1.12

1.12

1.00

1.12

0.99

1.05

1.00

1.05

0.99

0.93

1.00

0.92

1.00

0.72

1.08

0.87

1.10

1.12

1.00

1.11

1.00

0.99

1.00

1.02

1.00

1.07

1.00

1.07

1.00

Table 47. CMCRA (B6251) degradation ratios on replicates

Conditioning Step

External Heat without Agitation

External Heat with Mechanical Agitation

Frequency (rads/s)

5.0

50.0

5.0

50.0

5.0

50.0

5.0

50.0

Temperature

HT

HT

IT

IT

HT

HT

IT

IT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

0.69

1.02

0.82

1.11

1.13

1.01

1.12

0.99

1.02

1.01

1.00

0.98

0.96

1.00

0.95

0.99

0.90

0.98

0.93

1.03

1.14

1.00

1.13

0.99

1.02

1.01

1.01

0.99

0.98

1.00

0.97

1.00

-

-

-

-

1.18

1.00

1.17

0.99

1.04

1.00

1.00

0.98

0.96

1.00

0.95

1.00

24 hour

-

-

-

-

-

-

-

-

1.07

1.00

1.00

0.97

0.93

1.00

0.91

1.00

-

-

-

-

-

-

-

-

1.14

1.00

1.08

0.96

1.01

1.00

1.00

1.00

-

-

-

-

-

-

-

-

1.09

1.02

1.07

0.97

0.94

1.00

0.93

0.99

31 hour

1.03

0.96

0.99

1.00

1.06

0.99

1.04

0.99

1.27

1.01

1.20

0.93

0.97

0.99

0.96

0.99

1.01

0.97

1.03

1.00

1.17

1.00

1.14

0.99

1.00

0.99

0.91

0.69

1.00

0.99

0.98

0.99

0.95

0.99

0.96

1.02

1.20

0.99

1.17

0.98

-

-

-

-

1.01

0.99

0.99

0.99

48 hour

1.02

0.97

0.99

1.00

1.07

0.99

1.04

0.98

1.24

1.01

1.14

0.94

1.01

0.99

0.98

0.99

1.05

0.96

0.99

1.00

1.13

0.99

1.10

0.98

1.21

1.01

1.15

0.94

0.95

0.99

0.93

0.99

1.00

0.96

0.95

1.00

1.23

0.99

1.20

0.98

1.25

1.01

1.16

0.93

0.94

0.99

0.92

0.99


Table 48.  CMCRA (B6251) separation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

Time of Sampling

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

RS G*

RS delta symbol

0 hour

0.98

1.00

1.04

1.00

0.97

1.00

1.04

1.00

6 hour

0.84

1.02

0.90

1.03

0.90

1.05

0.96

1.03

0.84

1.01

0.91

1.01

0.90

1.04

0.94

1.02

-

-

-

-

-

-

-

-

24 hour

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

-

31 hour

0.61

1.09

-

-

0.78

1.14

-

-

0.72

1.07

-

-

0.89

1.10

-

-

0.68

1.07

-

-

0.84

1.11

-

-

48 hour

0.72

1.08

1.03

1.01

0.89

1.09

1.06

1.01

0.64

1.11

0.85

1.03

0.92

1.12

0.90

1.03

0.72

1.08

-

-

0.87

1.10

-

-

Table 49.  CMCRA (B6251) degradation ratios on replicate reruns

Conditioning Step

External Heat without Agitation

Frequency (rads/s)

5.0

5.0
Rerun

50.0

50.0
Rerun

Temperature

HT

HT

HT

HT

Time of Sampling

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

Rd G*

Rd delta symbol

0 hour

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

6 hour

0.69

1.02

0.99

0.98

0.82

1.11

0.97

0.99

0.90

0.98

0.92

0.99

0.93

1.03

0.91

1.00

-

-

-

-

-

-

-

-

24 hour

-

-

0.89

1.00

-

-

0.92

1.02

-

-

0.93

0.99

-

-

0.93

1.01

-

-

-

-

-

-

-

-

31 hour

1.03

0.96

-

-

0.99

1.00

-

-

1.01

0.97

-

-

1.03

1.00

-

-

0.95

0.99

-

-

0.96

1.02

-

-

48 hour

1.02

0.97

-

-

0.99

1.00

-

-

1.05

0.96

-

-

0.99

1.00

-

-

1.00

0.96

-

-

0.95

1.00

-

-

 

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