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Laboratory Overview | Laboratory Capabilities

 

 

Aggregate and Petrographic Laboratory

 

Laboratory Capabilities

Aggregate and Petrography

The Aggregate and Petrographic Laboratory characterizes and classifies aggregate types based upon their mineralogical makeup and physical characteristics of the rock types, and provides quantitative data for each rock type present in the aggregate in accordance with procedures set in American Society for Testing and Materials (ASTM) C 295. If aggregates are found to be of marginal or poor quality by petrography, additional durability, and performance testing is recommended in the analysis report.

the two images show stereomicroscope photographs of representative dense and porous chert particles from the materials retained on the No. 8 sieve size of the fine aggregate. The length of field of view in each image is 26 mm. The first image shows 6 dense chert particles, 3 particles on the top and 3 on the bottom. The second shows 5 porous particles. Three particles on the left and 2 particles on the right.
Figure 1a. Stereomicroscope photograph. Dense chert particles.

the two images show stereomicroscope photographs of representative dense and porous chert particles from the materials retained on the No. 8 sieve size of the fine aggregate. The length of field of view in each image is 26 mm. The first image shows 6 dense chert particles, 3 particles on the top and 3 on the bottom. The second shows 5 porous particles. Three particles on the left and 2 particles on the right.
Figure 1b. Stereomicroscope photograph. Porous and moderately soft chert particles.

 

Figure 1a and b. Stereomicroscope photographs of representative dense and porous chert particles from the materials retained on the No. 8 sieve size of  a fine aggregate. Length of field of view from left to right in each image is about 25 mm. Some chert materials in aggregates can affect performance in concrete, with respect to freeze-thaw damage or Alkali-Silica Reaction (ASR).

 

The image shows microcrystalline quartz, featuring a wavy black and cream-colored pattern.
Figure 2a. Photomicrograph. Fibrous Chalcedonic chert.

Figure 2b. Photomicrograph. Chalcedonic chert.
Figure 2b. Photomicrograph. Fibrous Chalcedonic chert.

 

Figure 2a and b.  Photomicrographs. Transmitted light (cross-polarized light), thin section photomicrographs of potentially ASR-reactive chalcedonic chert particles (microcrystalline quartz) from a fine aggregate. Note: accessory plate (gypsum) was inserted in b. Length of field of view from left to right in 2a is about 2 mm.

 

Concrete Petrography

The Aggregate and Petrographic Laboratory provides troubleshooting of performance problems and inferior quality, and investigates degradation and distress mechanisms of concrete and other materials from highway materials and concrete structures in accordance with procedures set in ASTM C 856. The laboratory also performs condition assessment and evaluates condition of: (a) concrete from existing structures by analyzing cores extracted from representative areas of the structure(s), and (b) concrete cylinders, prisms, and mortar bars subjected to strength and durability testing regimes.

Figure 3. Photomicrograph. Stereomicroscope photomicrograph of lapped and polished concrete section showing a translucent alkali-silica reaction (ASR) gel at the interface of a reactive chert coarse aggregate with the surrounding paste (shown by arrows).
Figure 3. Photomicrograph. Stereomicroscope photomicrograph of lapped and
polished concrete section showing a translucent ASR gel at the interface of
a reactive chert coarse aggregate with the surrounding paste (shown by arrows).

 

Figure 4. Photomicrograph. Stereomicroscope photomicrograph of lapped and polished concrete section showing ASR gel filled cracks radiating from a siliceous shale fine aggregate particle into the surrounding paste (shown by arrows).
Figure 4. Photomicrograph. Stereomicroscope photomicrograph of lapped and polished
concrete section showing ASR gel filled cracks radiating from a siliceous shale fine
aggregate particle into the surrounding paste (shown by arrows).

 

Figure 5a. Reactive siliceous limestone coarse aggregate.
Figure 5a. Reactive siliceous limestone coarse aggregate.

 

Figure 5b. Reactive siliceous shale fine aggregate.
Figure 5b. Reactive siliceous shale fine aggregate.

 

Figure 5a and b. Photomicrographs. Transmitted light (plane-polarized light) thin section photomicrographs showing cracks filled with ASR gel extending from reactive cherty limestone coarse aggregate (5a) and siliceous shale (5b) fine aggregate particles into the surrounding cement paste (shown by arrows).

Entrained Air-Void Systems in Concrete

The Aggregate and Petrographic Laboratory also evaluates and measures concrete air-void properties in accordance with procedures set in ASTM C 457. Air content and other air-void parameters (including spacing factor and specific surface) are critical to predict the freeze-thaw durability of concrete structures that will be or were exposed in different weathering regions.

Figure 6a. Photomicrograph. Lapped section of a concrete core showing the air-void system in a hardened concrete. The length of field of view from left to the right is approximately 9 mm.
Figure 6a. Photomicrograph. Lapped section of a concrete core showing the
air-void system in a hardened concrete. The length of field of view from
left to the right is approximately 9 mm.

 

Figure 6b. Photomicrograph. Stereomicroscope photograph of lapped section of concrete  after surface treatment was applied to perform RapidAir C457 air-void analysis.  The white spherical shapes are air voids in a hardened concrete.
Figure 6b. Photomicrograph. Stereomicroscope photograph of lapped section of
concrete after surface treatment was applied to perform RapidAir C457 air-void
analysis. The white spherical shapes are air voids in a hardened concrete.

 

Concrete Pavement

The Aggregate and Petrographic Laboratory helps in forensic investigations of problems relating to aggregate quality, low strength, Interfacial Transition Zone (ITZ), spalling and pop-outs, D-cracking, and Alkali-Aggregate Reaction (AAR).

Figure 7a. Stereophotomicrograph.
Figure 7a. Stereophotomicrograph.

 

Figure 7b. Stereophotomicrograph.
Figure 7b. Stereophotomicrograph.

 

Figure 7a and 7b. Stereophotomicrographs of altered and weathered volcanic rock aggregate particles in concrete exhibiting gaps at the interfaces within the cement paste. The gap/crack around a volcanic rock coarse aggregate is indicated by arrows. Also note the cracks within the coarse aggregate in 7a.

Figure 8a. Stereophotomicrograph.
Figure 8a. Stereophotomicrograph.

 

Figure 8b. Stereophotomicrograph.
Figure 8b. Stereophotomicrograph.

 

Figure 8a and 8b. Stereophotomicrographs of severely weathered and altered basalt fine aggregate particles showing gaps around the aggregates (yellow arrows) as well as internal cracks (red arrows). Notice the cracks in figure 8a developed along the light yellowish weathering rim/rind. Also, notice the intensity of internal cracks in the basalt particles in figure 8b (shown by red arrows).

Asphalt Pavement

The Aggregate and Petrographic Laboratory also helps in forensic investigations of problems related to aggregates in asphalt pavement, polishing/slipperiness issues of pavement surfaces, as well as examining sources and character of mineral fillers and other additions (e.g., lime) in  asphalt pavement mixtures.

Figure 9a. Photomicrograph. Very smooth and polished coarse aggregate from the middle  portion of a core extracted from an asphalt pavement.
Figure 9a. Photomicrograph. Very smooth and polished coarse aggregate from the middle portion of a core extracted from an asphalt pavement.

Figure 9b. Photomicrograph. Polished Aggregates (shown by arrows).
Figure 9b. Photomicrograph. Polished Aggregates (shown by arrows).

 

Figure 9a and 9b. Stereo-optical photomicrographs showing polished and smooth exposed aggregates along the top surface of a core extracted from an asphalt pavement. Scale shown in both images is in one-sixty-fourths-of-an-inch increment.

 

Figure 10a. Photomicrograph. Note the portion of the aggregate shown by red arrows is  still covered with asphaltic material.
Figure 10a. Photomicrograph. Note the portion of the aggregate shown by red arrows is still covered with asphaltic material.

Figure 10b. Photomicrograph. Middle portion is still covered with asphaltic materials  (shown by red arrows).
Figure 10b. Photomicrograph. Middle portion is still covered with asphaltic materials (shown by red arrows).

 

Figure 10a and 10b. Partially polished limestone aggregates (shown by yellow arrows). Broken yellow lines mark an inferred outline/edge of the aggregate particles in the portion where it is still covered by asphaltic material. Scale shown is in one-sixty-fourth-of-an-inch increment.

 

 

Federal Highway Administration | 1200 New Jersey Avenue, SE | Washington, DC 20590 | 202-366-4000
Turner-Fairbank Highway Research Center | 6300 Georgetown Pike | McLean, VA | 22101