U.S. Department of Transportation
Federal Highway Administration
1200 New Jersey Avenue, SE
Washington, DC 20590
202-366-4000
Federal Highway Administration Research and Technology
Coordinating, Developing, and Delivering Highway Transportation Innovations
 |
| This report is an archived publication and may contain dated technical, contact, and link information |
|
Publication Number: FHWA-HRT-04-111 Date: February 2005 |
Previous | Table of Contents | Next
Data deviating significantly from the average are highlighted.
Table 22. Elvaloy (B6228) separation ratios on replicates
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
0.95 |
1.00 |
1.03 |
1.00 |
0.93 |
1.00 |
0.93 |
1.00 |
1.00 |
1.00 |
0.98 |
1.00 |
1.76 |
1.00 |
1.75 |
1.00 |
6 hour |
0.96 |
1.00 |
0.98 |
1.01 |
1.00 |
1.00 |
1.00 |
1.00 |
0.95 |
1.00 |
0.96 |
1.01 |
1.07 |
1.00 |
1.08 |
1.00 |
1.04 |
1.00 |
1.02 |
0.99 |
1.08 |
1.00 |
1.11 |
1.01 |
0.91 |
1.00 |
0.91 |
1.04 |
1.15 |
1.00 |
1.16 |
1.00 |
|
1.01 |
0.66 |
0.99 |
1.00 |
1.01 |
1.00 |
1.03 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.02 |
1.00 |
1.01 |
0.98 |
|
24 hour |
0.98 |
1.00 |
0.99 |
1.00 |
0.97 |
1.00 |
0.97 |
1.00 |
0.99 |
1.00 |
0.97 |
1.01 |
1.22 |
0.97 |
1.18 |
0.99 |
1.01 |
1.00 |
1.00 |
1.00 |
1.02 |
1.00 |
1.01 |
1.00 |
0.96 |
1.00 |
0.98 |
1.01 |
1.04 |
1.00 |
1.05 |
1.00 |
|
0.97 |
1.00 |
0.98 |
1.01 |
0.90 |
1.00 |
0.90 |
1.00 |
0.93 |
1.01 |
0.97 |
1.02 |
0.93 |
1.00 |
0.93 |
1.00 |
|
31 hour |
1.02 |
1.00 |
1.00 |
1.00 |
0.94 |
1.00 |
0.93 |
1.00 |
1.10 |
1.01 |
1.09 |
0.97 |
1.11 |
1.00 |
1.13 |
1.00 |
1.01 |
1.00 |
1.01 |
0.99 |
1.22 |
1.00 |
1.23 |
1.00 |
0.96 |
1.00 |
0.97 |
1.01 |
0.94 |
1.00 |
0.95 |
1.00 |
|
1.02 |
1.00 |
0.98 |
1.00 |
1.05 |
1.00 |
1.05 |
1.00 |
0.97 |
1.00 |
0.97 |
1.00 |
0.96 |
1.00 |
0.96 |
0.99 |
|
48 hour |
1.00 |
0.99 |
0.97 |
1.01 |
0.96 |
1.00 |
0.96 |
1.00 |
0.93 |
1.00 |
0.98 |
1.02 |
1.06 |
1.00 |
1.04 |
0.99 |
0.92 |
1.01 |
0.93 |
1.03 |
0.76 |
1.01 |
0.78 |
1.00 |
0.99 |
1.00 |
0.99 |
1.00 |
0.96 |
1.00 |
0.96 |
1.00 |
|
1.00 |
1.00 |
1.01 |
1.00 |
0.91 |
1.00 |
0.92 |
1.00 |
0.91 |
1.00 |
0.93 |
1.02 |
1.01 |
1.00 |
1.01 |
1.00 |
|
Table 23. Elvaloy (B6228) degradation ratios on replicates
|
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
0 hour |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
6 hour |
0.81 |
1.04 |
0.92 |
1.06 |
0.91 |
1.00 |
0.90 |
1.00 |
0.88 |
1.03 |
0.96 |
1.04 |
0.96 |
1.00 |
0.96 |
1.00 |
0.74 |
1.04 |
0.87 |
1.09 |
0.80 |
1.00 |
0.79 |
0.99 |
0.89 |
1.03 |
0.97 |
1.04 |
1.00 |
1.00 |
1.00 |
1.00 |
|
0.79 |
1.31 |
0.91 |
1.07 |
0.84 |
1.00 |
0.84 |
0.99 |
0.89 |
1.03 |
0.97 |
1.03 |
0.98 |
1.00 |
0.99 |
1.01 |
|
24 hour |
0.80 |
1.05 |
0.93 |
1.07 |
1.02 |
0.99 |
1.01 |
0.99 |
0.88 |
1.05 |
0.99 |
1.03 |
0.96 |
0.98 |
0.94 |
0.99 |
0.78 |
1.04 |
0.92 |
1.08 |
0.98 |
0.99 |
0.96 |
0.99 |
0.89 |
1.05 |
1.00 |
1.03 |
0.96 |
1.00 |
0.96 |
0.99 |
|
0.79 |
1.04 |
0.94 |
1.07 |
0.87 |
0.99 |
0.85 |
0.99 |
0.91 |
1.05 |
1.02 |
1.03 |
0.98 |
0.99 |
0.96 |
0.99 |
|
31 hour |
0.86 |
1.03 |
0.98 |
1.04 |
0.96 |
0.99 |
0.94 |
0.99 |
0.92 |
1.04 |
1.02 |
1.03 |
1.02 |
0.99 |
1.01 |
0.99 |
0.85 |
1.03 |
0.98 |
1.04 |
0.93 |
0.99 |
0.91 |
0.99 |
0.90 |
1.05 |
1.00 |
1.03 |
0.93 |
0.99 |
0.91 |
0.99 |
|
0.85 |
1.03 |
0.98 |
1.05 |
0.98 |
0.99 |
0.97 |
0.99 |
0.94 |
1.05 |
1.05 |
1.02 |
1.03 |
0.99 |
1.01 |
0.99 |
|
48 hour |
0.98 |
1.01 |
1.08 |
1.00 |
0.96 |
0.99 |
0.94 |
0.98 |
0.98 |
1.04 |
1.08 |
1.00 |
1.02 |
0.99 |
1.00 |
0.99 |
0.94 |
1.02 |
1.03 |
1.01 |
1.08 |
0.98 |
1.05 |
0.98 |
0.98 |
1.04 |
1.08 |
1.00 |
1.01 |
0.99 |
1.00 |
0.98 |
|
0.95 |
1.01 |
1.04 |
1.01 |
0.89 |
0.98 |
0.86 |
0.98 |
0.92 |
1.04 |
1.03 |
1.03 |
0.99 |
0.98 |
0.97 |
0.98 |
|
Table 24. Elvaloy (B6228) separation ratios on replicate reruns
Conditioning Step |
External Heat without Agitation |
|||||||
|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
5.0 |
50.0 |
50.0 |
||||
Temperature |
HT |
HT |
HT |
HT |
||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
0.95 |
1.00 |
- |
- |
1.03 |
1.00 |
- |
- |
6 hour |
0.96 |
1.00 |
1.04 |
1.00 |
0.98 |
1.01 |
1.03 |
1.00 |
1.04 |
1.00 |
1.00 |
1.00 |
1.02 |
0.99 |
1.00 |
1.00 |
|
1.01 |
0.66 |
- |
- |
0.99 |
1.00 |
- |
- |
|
24 hour |
0.98 |
1.00 |
0.97 |
1.01 |
0.99 |
1.00 |
0.98 |
1.00 |
1.01 |
1.00 |
1.02 |
1.00 |
1.00 |
1.00 |
1.01 |
1.00 |
|
0.97 |
1.00 |
- |
- |
0.98 |
1.01 |
- |
- |
|
31 hour |
1.02 |
1.00 |
1.05 |
0.99 |
1.00 |
1.00 |
1.04 |
1.00 |
1.01 |
1.00 |
0.96 |
1.00 |
1.01 |
0.99 |
0.97 |
1.00 |
|
1.02 |
1.00 |
- |
- |
0.98 |
1.00 |
- |
- |
|
48 hour |
1.00 |
0.99 |
0.97 |
1.00 |
0.97 |
1.01 |
0.97 |
1.00 |
0.92 |
1.01 |
- |
- |
0.93 |
1.03 |
- |
- |
|
1.00 |
1.00 |
- |
- |
1.01 |
1.00 |
- |
- |
|
Table 25. Elvaloy (B6228) degradation ratios on replicate reruns
Conditioning Step |
External Heat without Agitation |
|||||||
Frequency (rads/s) |
5.0 |
5.0 |
50.0 | 50.0 |
||||
|---|---|---|---|---|---|---|---|---|
Temperature |
HT |
HT |
HT |
HT |
||||
Time of Sampling |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
0 hour |
1.00 |
1.00 |
- |
- |
1.00 |
1.00 |
- |
- |
6 hour |
0.81 |
1.04 |
0.88 |
1.03 |
0.92 |
1.06 |
1.00 |
0.93 |
0.74 |
1.04 |
0.86 |
1.03 |
0.87 |
1.09 |
0.90 |
1.02 |
|
0.79 |
1.31 |
- |
- |
0.91 |
1.07 |
- |
- |
|
24 hour |
0.80 |
1.05 |
0.86 |
1.04 |
0.93 |
1.07 |
0.92 |
1.03 |
0.78 |
1.04 |
0.87 |
1.04 |
0.92 |
1.08 |
0.93 |
1.03 |
|
0.79 |
1.04 |
- |
- |
0.94 |
1.07 |
- |
- |
|
31 hour |
0.86 |
1.03 |
0.90 |
1.03 |
0.98 |
1.04 |
0.95 |
1.03 |
0.85 |
1.03 |
0.86 |
1.03 |
0.98 |
1.04 |
0.92 |
1.03 |
|
0.85 |
1.03 |
- |
- |
0.98 |
1.05 |
- |
- |
|
48 hour |
0.98 |
1.01 |
0.94 |
1.02 |
1.08 |
1.00 |
0.98 |
1.02 |
0.94 |
1.02 |
- |
- |
1.03 |
1.01 |
- |
- |
|
0.95 |
1.01 |
- |
- |
1.04 |
1.01 |
- |
- |
|
Table 26. SBS-lg (B6229) separation ratios on replicates
|
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
1.0 |
1.00 |
0.99 |
1.00 |
1.04 |
1.00 |
1.04 |
1.00 |
0.93 |
1.02 |
1.01 |
1.01 |
1.03 |
1.01 |
1.03 |
1.01 |
6 hour |
1.02 |
0.99 |
1.00 |
1.00 |
1.3 |
0.99 |
1.01 |
0.99 |
0.89 |
1.01 |
0.92 |
1.03 |
0.96 |
1.01 |
0.98 |
1.01 |
0.93 |
0.99 |
0.95 |
1.02 |
1.13 |
1.00 |
1.11 |
1.00 |
0.97 |
0.99 |
0.97 |
1.01 |
0.89 |
1.00 |
0.89 |
1.00 |
|
24 hour |
1.04 |
0.99 |
1.02 |
1.00 |
1.51 |
1.03 |
1.60 |
1.03 |
0.97 |
0.97 |
0.96 |
1.01 |
0.75 |
1.00 |
0.76 |
1.00 |
0.97 |
1.02 |
1.01 |
1.00 |
0.99 |
1.01 |
1.00 |
1.00 |
0.98 |
1.01 |
0.99 |
1.01 |
1.10 |
1.00 |
1.10 |
1.00 |
|
31 hour |
1.03 |
1.02 |
1.04 |
0.99 |
1.09 |
1.01 |
1.11 |
1.01 |
1.02 |
0.97 |
1.00 |
1.00 |
1.13 |
1.00 |
1.13 |
1.00 |
1.01 |
0.99 |
0.99 |
1.00 |
1.05 |
1.01 |
1.05 |
1.00 |
0.94 |
1.01 |
0.99 |
1.01 |
1.06 |
1.00 |
1.07 |
1.00 |
|
48 hour |
0.70 |
1.01 |
0.92 |
1.00 |
0.79 |
0.99 |
0.78 |
0.99 |
0.99 |
1.02 |
1.01 |
1.00 |
1.01 |
1.00 |
1.00 |
1.00 |
2.67 |
0.95 |
2.37 |
0.79 |
1.02 |
1.00 |
1.02 |
1.00 |
1.00 |
0.99 |
1.00 |
0.97 |
0.98 |
1.00 |
0.98 |
1.00 |
|
Table 27. SBS-lg (B6229) degradation ratios on replicates
|
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
0 hour |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
6 hour |
1.08 |
1.01 |
1.03 |
0.98 |
0.93 |
0.98 |
0.90 |
0.99 |
1.01 |
1.01 |
1.01 |
0.99 |
1.05 |
1.00 |
1.05 |
1.00 |
1.05 |
1.02 |
1.02 |
0.99 |
0.97 |
0.98 |
0.94 |
0.99 |
1.04 |
1.01 |
1.04 |
0.97 |
1.06 |
1.00 |
1.05 |
0.99 |
|
24 hour |
1.16 |
1.00 |
1.04 |
0.96 |
0.78 |
0.99 |
0.76 |
0.99 |
1.11 |
0.98 |
1.02 |
0.96 |
1.00 |
1.00 |
0.99 |
1.00 |
1.16 |
0.98 |
1.03 |
0.96 |
1.01 |
1.00 |
1.01 |
1.00 |
1.13 |
0.99 |
1.05 |
0.96 |
0.95 |
1.00 |
0.95 |
1.00 |
|
31 hour |
1.26 |
0.95 |
1.04 |
0.94 |
0.93 |
1.00 |
0.92 |
1.00 |
1.16 |
0.97 |
1.02 |
0.96 |
1.03 |
1.01 |
1.03 |
1.00 |
1.20 |
0.97 |
1.03 |
0.94 |
1.01 |
1.00 |
1.00 |
1.00 |
1.18 |
0.98 |
1.04 |
0.95 |
1.01 |
1.01 |
1.02 |
1.00 |
|
48 hour |
6.94 |
0.88 |
3.93 |
0.67 |
0.84 |
0.99 |
0.83 |
1.00 |
1.24 |
0.91 |
0.98 |
0.94 |
1.00 |
1.01 |
1.02 |
1.01 |
2.63 |
0.92 |
1.84 |
0.81 |
0.93 |
1.00 |
0.92 |
1.00 |
1.23 |
0.94 |
1.00 |
0.94 |
0.95 |
1.01 |
0.97 |
1.01 |
|
Table 28. SBS-lg (B6229) separation ratios on replicate reruns
Conditioning Step |
External Heat without Agitation |
|||||||
|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
5.0 |
50.0 |
50.0 |
||||
Temperature |
HT |
HT |
HT |
HT |
||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
1.0 |
1.00 |
1.04 |
1.01 |
0.99 |
1.00 |
1.04 |
1.00 |
6 hour |
1.02 |
0.99 |
0.84 |
1.00 |
1.00 |
1.00 |
0.84 |
1.01 |
0.93 |
0.99 |
1.00 |
0.99 |
0.95 |
1.02 |
1.00 |
1.00 |
|
24 hour |
1.04 |
0.99 |
0.95 |
0.99 |
1.02 |
1.00 |
0.94 |
1.00 |
0.97 |
1.02 |
0.99 |
0.99 |
1.01 |
1.00 |
0.98 |
1.00 |
|
31 hour |
1.03 |
1.02 |
- |
- |
1.04 |
0.99 |
- |
- |
1.01 |
0.99 |
- |
- |
0.99 |
1.00 |
- |
- |
|
48 hour |
0.70 |
1.01 |
1.03 |
1.00 |
0.92 |
1.00 |
1.03 |
1.00 |
2.67 |
0.95 |
0.98 |
1.00 |
2.37 |
0.79 |
0.97 |
1.00 |
|
Table 29. SBS-lg (B6229) degradation ratios on replicate reruns
Conditioning Step |
External Heat without Agitation |
|||||||
|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
5.0 |
50.0 |
50.0 |
||||
Temperature |
HT |
HT |
HT |
HT |
||||
Time of Sampling |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
0 hour |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
6 hour |
1.08 |
1.01 |
0.89 |
1.03 |
1.03 |
0.98 |
0.90 |
1.00 |
1.05 |
1.02 |
0.94 |
1.02 |
1.02 |
0.99 |
0.96 |
1.00 |
|
24 hour |
1.16 |
1.00 |
1.00 |
1.00 |
1.04 |
0.96 |
0.95 |
0.97 |
1.16 |
0.98 |
1.07 |
0.99 |
1.03 |
0.96 |
1.00 |
0.97 |
|
31 hour |
1.26 |
0.95 |
- |
- |
1.04 |
0.94 |
- |
- |
1.20 |
0.97 |
- |
- |
1.03 |
0.94 |
- |
- |
|
48 hour |
6.94 |
0.88 |
1.17 |
0.94 |
3.93 |
0.67 |
1.01 |
0.94 |
2.63 |
0.92 |
1.21 |
0.92 |
1.84 |
0.81 |
1.03 |
0.93 |
|
Table 30. SBS-l (B6230) separation ratios on replicates
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
1.13 |
0.98 |
1.10 |
0.99 |
0.96 |
1.00 |
0.97 |
1.01 |
1.07 |
0.98 |
1.06 |
1.00 |
- |
- |
- |
- |
6 hour |
1.03 |
0.98 |
1.01 |
0.98 |
0.89 |
0.97 |
0.84 |
0.97 |
0.99 |
1.03 |
1.04 |
1.02 |
1.08 |
1.01 |
1.10 |
1.01 |
1.02 |
0.99 |
1.01 |
1.00 |
1.05 |
1.01 |
1.08 |
1.01 |
0.93 |
1.04 |
1.00 |
1.02 |
1.11 |
1.01 |
1.12 |
1.01 |
|
1.04 |
1.01 |
1.02 |
0.99 |
- |
- |
- |
- |
0.97 |
0.99 |
0.97 |
1.00 |
0.95 |
1.00 |
0.94 |
0.99 |
|
24 hour |
1.01 |
1.00 |
1.02 |
1.00 |
0.94 |
0.98 |
0.91 |
0.98 |
0.99 |
0.99 |
0.99 |
1.01 |
0.93 |
1.00 |
0.94 |
1.00 |
0.94 |
1.00 |
0.94 |
1.00 |
1.14 |
0.99 |
1.13 |
0.99 |
1.03 |
0.99 |
1.00 |
1.01 |
1.04 |
1.00 |
1.05 |
1.00 |
|
1.06 |
1.00 |
1.04 |
0.99 |
0.94 |
1.00 |
0.94 |
1.00 |
0.93 |
1.04 |
0.98 |
1.02 |
0.97 |
1.01 |
0.97 |
1.01 |
|
31 hour |
0.97 |
1.01 |
1.01 |
1.02 |
1.03 |
1.00 |
1.04 |
1.00 |
1.01 |
1.01 |
1.03 |
1.00 |
1.02 |
1.01 |
1.03 |
1.01 |
1.01 |
0.98 |
0.98 |
0.99 |
1.01 |
1.01 |
1.04 |
1.01 |
0.98 |
1.04 |
0.97 |
1.01 |
1.13 |
1.00 |
1.13 |
0.99 |
|
0.96 |
1.01 |
0.96 |
1.00 |
1.08 |
1.02 |
1.12 |
1.02 |
- |
- |
- |
- |
1.00 |
1.00 |
0.99 |
1.00 |
|
48 hour |
0.92 |
1.02 |
0.96 |
1.02 |
0.84 |
1.01 |
0.85 |
1.01 |
1.06 |
0.99 |
1.04 |
1.01 |
0.94 |
1.00 |
0.96 |
1.00 |
0.96 |
1.00 |
0.96 |
1.01 |
0.98 |
1.01 |
0.98 |
1.00 |
1.01 |
0.98 |
0.99 |
1.00 |
1.16 |
1.00 |
1.15 |
1.00 |
|
1.04 |
1.00 |
1.04 |
1.00 |
0.99 |
1.00 |
0.99 |
1.00 |
1.01 |
1.00 |
1.00 |
1.00 |
1.11 |
1.00 |
1.11 |
1.00 |
|
Table 31. SBS-l (B6230) degradation ratios on replicates
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
0 hour |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
- |
- |
- |
- |
6 hour |
1.22 |
1.02 |
1.20 |
0.96 |
0.92 |
0.97 |
0.88 |
0.97 |
1.11 |
0.99 |
1.07 |
0.97 |
1.11 |
0.99 |
1.11 |
0.90 |
1.24 |
1.02 |
1.22 |
0.97 |
0.98 |
0.97 |
0.94 |
0.98 |
1.08 |
1.01 |
1.05 |
0.98 |
1.17 |
0.99 |
1.15 |
0.89 |
|
1.18 |
1.02 |
1.18 |
0.97 |
- |
- |
- |
- |
1.05 |
1.00 |
1.03 |
0.98 |
1.15 |
0.99 |
1.13 |
0.89 |
|
24 hour |
1.13 |
1.01 |
1.07 |
0.96 |
0.89 |
0.98 |
0.85 |
0.98 |
1.24 |
0.95 |
1.07 |
0.93 |
1.02 |
1.00 |
1.02 |
0.99 |
1.11 |
1.01 |
1.07 |
0.96 |
0.93 |
0.98 |
0.91 |
0.99 |
1.20 |
0.95 |
1.05 |
0.94 |
1.02 |
0.99 |
1.02 |
0.90 |
|
1.14 |
1.02 |
1.10 |
0.97 |
0.88 |
0.98 |
0.85 |
0.99 |
1.22 |
0.94 |
1.05 |
0.93 |
1.04 |
1.00 |
1.04 |
0.91 |
|
31 hour |
1.17 |
1.01 |
1.11 |
0.96 |
0.94 |
0.98 |
0.9 |
0.98 |
1.25 |
0.96 |
1.10 |
0.93 |
1.11 |
1.00 |
1.10 |
0.90 |
1.12 |
1.03 |
1.09 |
0.97 |
0.93 |
0.96 |
0.88 |
0.97 |
1.27 |
0.94 |
1.10 |
0.93 |
1.02 |
1.00 |
1.02 |
0.91 |
|
1.15 |
1.02 |
1.11 |
0.96 |
0.88 |
0.96 |
0.83 |
0.97 |
- |
- |
- |
- |
1.10 |
1.00 |
1.10 |
0.91 |
|
48 hour |
1.27 |
1.00 |
1.17 |
0.94 |
0.94 |
0.98 |
0.91 |
0.98 |
1.28 |
0.94 |
1.04 |
0.90 |
1.13 |
1.00 |
1.13 |
0.90 |
1.21 |
1.02 |
1.13 |
0.95 |
1.01 |
0.98 |
0.98 |
0.98 |
1.23 |
0.94 |
1.01 |
0.91 |
1.09 |
1.00 |
1.09 |
0.91 |
|
1.20 |
1.01 |
1.13 |
0.95 |
0.95 |
0.98 |
0.93 |
0.98 |
1.27 |
0.94 |
1.04 |
0.91 |
1.13 |
1.00 |
1.13 |
0.91 |
|
Table 32. SBS-rg (B6231) separation ratios on replicates
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
0.86 |
1.01 |
0.96 |
1.03 |
1.04 |
1.00 |
1.04 |
1.00 |
0.86 |
1.02 |
0.91 |
1.04 |
0.99 |
1.01 |
1.00 |
1.00 |
6 hour |
1.23 |
1.01 |
1.11 |
0.98 |
1.10 |
1.00 |
1.11 |
1.00 |
0.92 |
1.01 |
0.89 |
1.00 |
3.89 |
1.22 |
6.41 |
1.17 |
0.62 |
0.98 |
0.98 |
0.98 |
0.90 |
1.00 |
0.90 |
1.01 |
1.53 |
1.01 |
0.94 |
1.01 |
0.96 |
1.00 |
0.97 |
1.00 |
|
24 hour |
1.06 |
0.99 |
1.11 |
0.99 |
1.03 |
0.99 |
1.02 |
0.99 |
0.94 |
0.98 |
1.02 |
1.00 |
0.98 |
1.00 |
0.98 |
1.00 |
1.03 |
0.96 |
0.97 |
0.99 |
0.91 |
1.01 |
0.93 |
1.01 |
0.99 |
1.00 |
0.97 |
1.00 |
1.14 |
1.00 |
1.14 |
0.99 |
|
31 hour |
1.05 |
0.98 |
0.97 |
0.99 |
1.08 |
1.00 |
1.08 |
1.00 |
0.92 |
0.98 |
0.91 |
1.02 |
1.10 |
1.02 |
1.15 |
1.03 |
1.09 |
0.99 |
1.05 |
0.97 |
1.11 |
0.99 |
1.10 |
1.00 |
1.10 |
0.98 |
1.02 |
0.98 |
0.99 |
1.00 |
1.00 |
1.00 |
|
48 hour |
1.00 |
0.98 |
0.98 |
1.00 |
0.96 |
1.00 |
0.96 |
1.00 |
0.97 |
1.00 |
0.95 |
1.02 |
0.99 |
1.00 |
0.98 |
1.00 |
1.28 |
0.99 |
1.04 |
0.98 |
1.15 |
1.01 |
1.17 |
1.00 |
0.26 |
0.99 |
1.02 |
0.99 |
0.92 |
1.00 |
0.92 |
1.00 |
|
Table 33. SBS-rg (B6231) degradation ratios on replicates
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
5.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
IT |
IT |
HT |
HT |
IT |
IT |
||||||||
Time of Sampling |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
Rd G* |
Rd |
0 hour |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
1.00 |
6 hour |
1.50 |
0.95 |
1.1 |
0.9 |
0.99 |
0.96 |
0.94 |
0.96 |
1.05 |
1.03 |
1.14 |
0.99 |
0.58 |
0.91 |
0.54 |
0.93 |
2.04 |
0.94 |
1.16 |
0.87 |
0.9 |
0.96 |
0.86 |
0.97 |
1.38 |
1.03 |
1.15 |
0.99 |
1.04 |
1.01 |
1.05 |
1.01 |
|
24 hour |
1.31 |
0.94 |
1.05 |
0.92 |
0.79 |
0.97 |
0.77 |
0.98 |
1.19 |
1.00 |
1.10 |
0.98 |
1.01 |
1.01 |
1.03 |
1.01 |
1.31 |
0.94 |
1.00 |
0.91 |
0.83 |
0.98 |
0.82 |
0.99 |
1.11 |
1.00 |
1.08 |
0.98 |
0.92 |
1.01 |
0.94 |
1.01 |
|
31 hour |
1.31 |
0.94 |
0.99 |
0.91 |
0.86 |
0.97 |
0.84 |
0.98 |
1.10 |
0.99 |
1.07 |
0.98 |
0.79 |
1.00 |
0.80 |
1.00 |
1.28 |
0.94 |
0.96 |
0.92 |
0.85 |
0.97 |
0.83 |
0.98 |
1.14 |
1.00 |
1.11 |
0.98 |
1.00 |
1.01 |
1.02 |
1.01 |
|
48 hour |
1.31 |
0.94 |
0.97 |
0.92 |
0.84 |
0.98 |
0.83 |
0.99 |
1.17 |
0.98 |
1.10 |
0.97 |
0.95 |
1.01 |
0.97 |
1.01 |
1.40 |
0.94 |
0.99 |
0.91 |
0.85 |
0.98 |
0.85 |
0.99 |
2.29 |
0.97 |
1.10 |
0.96 |
0.85 |
1.01 |
0.86 |
1.01 |
|
Table 34. SBS-rg (B6231) separation ratios on replicate reruns
Conditioning Step |
External Heat without Agitation |
External Heat with Mechanical Agitation |
||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Frequency (rads/s) |
5.0 |
5.0 |
50.0 | 50.0 Rerun |
5.0 |
5.0 |
50.0 |
50.0 |
||||||||
Temperature |
HT |
HT |
HT |
HT |
HT |
HT |
HT |
HT |
||||||||
Time of Sampling |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
RS G* |
RS |
0 hour |
0.86 |
1.01 |
1.19 |
0.99 |
0.96 |
1.03 |
1.19 |
0.99 |
0.86 |
1.02 |
1.03 |
0.99 |
0.91 |
1.04 |
1.02 |
1.00 |
6 hour |
1.23 |
1.01 |
1.12 |
0.97 |
1.11 |
0.98 |
1.06 |
0.98 |
0.92 |
1.01 |
1.03 |
0.99 |
0.89 |
1.00 |
0.99 |
0.98 |
0.62 |
0.98 |
1.11 |
0.98 |
0.98 |
0.98 |
1.05 |
0.97 |
1.53 |
1.01 |
1.12 |
0.99 |
0.94 |
1.01 |
1.06 |
0.97 |
|
24 hour |
1.06 |
0.99 |
1.00 |
0.98 |
1.11 |
0.99 |
0.96 |
0.99 |
0.94 |
0.98 |
1.01 |
1.00 |
1.02 |
1.00 |
1.01 |
1.00 |
1.03 |
0.96 |
1.11 |
0.97 |
0.97 |
0.99 |
1.07 |
0.99 |
0.99 |
1.00 |
0.97 |
1.00 |
0.97 |
1.00 |
0.97 |
1.00 |
|
31 hour |
1.05 |
0.98 |
- |
- |
0.97 |
0.99 |
- |
- |
0.92 |
0.98 |
- |
- |
0.91 |
1.02 |
- |
- |
1.09 |
0.99 |
- |
- |
1.05 |
0.97 |
- |
- |
1.10 |
0.98 |
- |
- |
1.02 |
0.98 |
- |
- |
|
48 hour |
1.00 |
0.98 |
1.09 |
0.99 |
0.98 |
1.00 |
1.07 |
1.00 |
0.97 |
1.00 |
1.03 |
0.99 |
0.95 |
1.02 |
1.01 |
1.00 |
1.28 |
0.99 |
0.98 |
1.00 |
1.04 |
0.98 |
0.97 |
1.00 |
0.26 |
0.99 |
0.96 |
1.00 |
1.02 |
0.99 |
0.96 |
1.00 |
|
